Influence of Carbon and Scandium on Structure of Metastable Al$_3$Mg Phase and Properties of SPS-Composites
A. D. Rud$^{1}$, A. M. Lakhnik$^{1}$, I. M. Kirian$^{1}$, O. N. Syzonenko$^{2}$, N. S. Prystash$^{2}$, S. O. Demchenkov$^{3}$, Yu. V. Lepeeva$^{1}$
$^{1}$G. V. Kurdyumov Institute for Metal Physics, NAS of Ukraine, 36 Academician Vernadsky Blvd., UA-03142 Kyiv, Ukraine
$^{2}$Institute of Pulse Processes and Technologies, N.A.S. of Ukraine, 43А Bohoyavlensky Ave., UA-54018 Mykolaiv, Ukraine
$^{3}$E. O. Paton Electric Welding Institute, NAS of Ukraine, 11 Kazymyr Malevych Str., UA-03150 Kyiv, Ukraine
Received: 13.04.2021; final version - 14.06.2021. Download: PDF
The solid dispersant (graphite) and additional alloying by scandium effects on the intermetallic compound formation in the Al–Mg system under mechanical alloying are studied. As found, the scandium additive significantly accelerates the metastable intermetallic Al$_3$Mg phase formation in (75% at. (Al + 2% wt. Sc)–25% at. Mg)/5% wt. C powder mixture compared to the (75% at. Al–25% at. Mg )/5% wt. C one. The synthesized powder composite, containing metastable Al$_3$Mg phase and solid solution based on aluminium, is consolidated by the spark plasma sintering (SPS) method. The phase composition, structure, and hardness of the SPS sintered samples are determined by X-ray diffraction, scanning electron microscopy, and indentation by the Vickers indenter. The hardness of samples formed after spark plasma sintering is in the range of 175–212 $HV$ and significantly exceeds the hardness of duralumin (124 $HV$).
Key words: aluminium-magnesium alloys, metastable Al$_3$Mg intermetallic compound, mechanical alloying, spark plasma sintering (SPS).
URL: https://mfint.imp.kiev.ua/en/abstract/v43/i08/1045.html
DOI: https://doi.org/10.15407/mfint.43.08.1045
PACS: 61.05.cp, 64.60.My, 68.35.Dv, 81.20.Ev
Citation: A. D. Rud, A. M. Lakhnik, I. M. Kirian, O. N. Syzonenko, N. S. Prystash, S. O. Demchenkov, and Yu. V. Lepeeva, Influence of Carbon and Scandium on Structure of Metastable Al$_3$Mg Phase and Properties of SPS-Composites, Metallofiz. Noveishie Tekhnol., 43, No. 8: 1045—1052 (2021)