Issues »  Volume 45, Issue 10

Single-Step Pressureless Synthesis of the High-Purity Ti$_{3}$AlC$_{2}$ MAX-Phase by Fast Heating

I. M. Kirian$^{1}$, A. M. Lakhnik$^{1}$, O. Yu. Khyzhun$^{2}$, I. V. Zagorulko$^{1}$, A. S. Nikolenko$^{3}$, O. D. Rud’$^{1}$

$^{1}$G. V. Kurdyumov Institute for Metal Physics, NAS of Ukraine, 36 Academician Vernadsky Blvd., UA-03142 Kyiv, Ukraine
$^{2}$I. M. Frantsevich Institute for Problems in Materials Science, NAS of Ukraine, 3 Omeljan Pritsak Str., UA-03142 Kyiv, Ukraine
$^{3}$V. E. Lashkaryov Institute of Semiconductor Physics, NAS of Ukraine, 41 Nauky Ave., UA-03028 Kyiv, Ukraine

Received: 03.07.2023; final version - 19.09.2023. Download: PDF

A simple approach is presented to synthesise the high-purity MAX phase by the pressureless method. This method is featured by the short time in duration. The process is executed with a high heating rate (up to $\cong 10^{2}$ K/min) that inhibits the formation of the objectionable phases and limits elemental loss due to the short-time process. The samples containing $\cong$ 96% wt. of the MAX phase Ti$_{3}$AlC$_{2}$ are successfully synthesised using the proposed technique.

Key words: MAX phase, pressureless synthesis, fast heating, ball milling.

URL: https://mfint.imp.kiev.ua/en/abstract/v45/i10/1165.html

DOI: https://doi.org/10.15407/mfint.45.10.1165

PACS: 61.05.cp, 77.84.Bw, 78.30.Hv, 81.05.Je, 81.20.Ev, 81.20.Wk, 82.80.Pv

Citation: I. M. Kirian, A. M. Lakhnik, O. Yu. Khyzhun, I. V. Zagorulko, A. S. Nikolenko, and O. D. Rud’, Single-Step Pressureless Synthesis of the High-Purity Ti$_{3}$AlC$_{2}$ MAX-Phase by Fast Heating, Metallofiz. Noveishie Tekhnol., 45, No. 10: 1165—1177 (2023)

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