Processing math: 100%
Issues »  Volume 45, Issue 10

Single-Step Pressureless Synthesis of the High-Purity Ti3AlC2 MAX-Phase by Fast Heating

I. M. Kirian1, A. M. Lakhnik1, O. Yu. Khyzhun2, I. V. Zagorulko1, A. S. Nikolenko3, O. D. Rud’1

1G. V. Kurdyumov Institute for Metal Physics, NAS of Ukraine, 36 Academician Vernadsky Blvd., UA-03142 Kyiv, Ukraine
2I. M. Frantsevich Institute for Problems in Materials Science, NAS of Ukraine, 3 Omeljan Pritsak Str., UA-03142 Kyiv, Ukraine
3V. E. Lashkaryov Institute of Semiconductor Physics, NAS of Ukraine, 41 Nauky Ave., UA-03028 Kyiv, Ukraine

Received: 03.07.2023; final version - 19.09.2023. Download: PDF

A simple approach is presented to synthesise the high-purity MAX phase by the pressureless method. This method is featured by the short time in duration. The process is executed with a high heating rate (up to ≅102 K/min) that inhibits the formation of the objectionable phases and limits elemental loss due to the short-time process. The samples containing ≅ 96% wt. of the MAX phase Ti3AlC2 are successfully synthesised using the proposed technique.

Key words: MAX phase, pressureless synthesis, fast heating, ball milling.

URL: https://mfint.imp.kiev.ua/en/abstract/v45/i10/1165.html

DOI: https://doi.org/10.15407/mfint.45.10.1165

PACS: 61.05.cp, 77.84.Bw, 78.30.Hv, 81.05.Je, 81.20.Ev, 81.20.Wk, 82.80.Pv

Citation: I. M. Kirian, A. M. Lakhnik, O. Yu. Khyzhun, I. V. Zagorulko, A. S. Nikolenko, and O. D. Rud’, Single-Step Pressureless Synthesis of the High-Purity Ti3AlC2 MAX-Phase by Fast Heating, Metallofiz. Noveishie Tekhnol., 45, No. 10: 1165—1177 (2023)

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