Выпуски МФиНТ »  Том 45, выпуск 10

Single-Step Pressureless Synthesis of the High-Purity Ti$_{3}$AlC$_{2}$ MAX-Phase by Fast Heating

I. M. Kirian$^{1}$, A. M. Lakhnik$^{1}$, O. Yu. Khyzhun$^{2}$, I. V. Zagorulko$^{1}$, A. S. Nikolenko$^{3}$, O. D. Rud’$^{1}$

$^{1}$Институт металлофизики им. Г. В. Курдюмова НАН Украины, бульв. Академика Вернадского, 36, 03142 Киев, Украина
$^{2}$Институт проблем материаловедения им. И. Н. Францевича НАН Украины, ул. Омельяна Прицака, 3, 03142 Киев, Украина
$^{3}$Институт физики полупроводников им. В. Е. Лашкарёва НАН Украины, просп. Науки, 41, 03028 Киев, Украина

Получена: 03.07.2023; окончательный вариант - 19.09.2023. Скачать: PDF

A simple approach is presented to synthesise the high-purity MAX phase by the pressureless method. This method is featured by the short time in duration. The process is executed with a high heating rate (up to $\cong 10^{2}$ K/min) that inhibits the formation of the objectionable phases and limits elemental loss due to the short-time process. The samples containing $\cong$ 96% wt. of the MAX phase Ti$_{3}$AlC$_{2}$ are successfully synthesised using the proposed technique.

Ключевые слова: MAX phase, pressureless synthesis, fast heating, ball milling.

URL: https://mfint.imp.kiev.ua/ru/abstract/v45/i10/1165.html

PACS: 61.05.cp, 77.84.Bw, 78.30.Hv, 81.05.Je, 81.20.Ev, 81.20.Wk, 82.80.Pv

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