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Single-Step Pressureless Synthesis of the High-Purity Ti3AlC2 MAX-Phase by Fast Heating

I. M. Kirian1, A. M. Lakhnik1, O. Yu. Khyzhun2, I. V. Zagorulko1, A. S. Nikolenko3, O. D. Rud’1

1Институт металлофизики им. Г. В. Курдюмова НАН Украины, бульв. Академика Вернадского, 36, 03142 Киев, Украина
2Институт проблем материаловедения им. И. Н. Францевича НАН Украины, ул. Омельяна Прицака, 3, 03142 Киев, Украина
3Институт физики полупроводников им. В. Е. Лашкарёва НАН Украины, просп. Науки, 41, 03028 Киев, Украина

Получена: 03.07.2023; окончательный вариант - 19.09.2023. Скачать: PDF

A simple approach is presented to synthesise the high-purity MAX phase by the pressureless method. This method is featured by the short time in duration. The process is executed with a high heating rate (up to 102 K/min) that inhibits the formation of the objectionable phases and limits elemental loss due to the short-time process. The samples containing 96% wt. of the MAX phase Ti3AlC2 are successfully synthesised using the proposed technique.

Ключевые слова: MAX phase, pressureless synthesis, fast heating, ball milling.

URL: https://mfint.imp.kiev.ua/ru/abstract/v45/i10/1165.html

PACS: 61.05.cp, 77.84.Bw, 78.30.Hv, 81.05.Je, 81.20.Ev, 81.20.Wk, 82.80.Pv


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